Extraction and Solubility Modeling of Anthocyanins Rich Extract from Hibiscus sabdariffa L. using Supercritical Carbon Dioxide

Zuhaili Idham; Nicky Rahmana Putra; Hasmida Nasir; Lee Nian Yian; Nor Faadila Mohd Idrus; Mohd Azizi Che Yunus

doi:10.11113/mjfas.v17n6.2285

Authors

Zuhaili Idham Universiti Teknologi Malaysia https://orcid.org/0000-0003-2049-6245
Nicky Rahmana Putra Universiti Teknologi Malaysia
Hasmida Nasir Universiti Teknologi Malaysia
Lee Nian Yian Universiti Teknologi Malaysia
Nor Faadila Mohd Idrus Universiti Teknologi Malaysia
Mohd Azizi Che Yunus Universiti Teknologi Malaysia

DOI:

https://doi.org/10.11113/mjfas.v17n6.2285

Keywords:

Hibiscus sabdariffa, Anthocyanins, Supercritical carbon dioxide, solubility, modeling,

Abstract

This study aimed to evaluate the extraction yield, and anthocyanins content of Hibiscus sabdariffa L. calyces extract using different temperatures (T) at 50 - 70°C, pressure (P) at 8 - 12 MPa, and modifier ratio at 5 - 10%. This work used a supercritical carbon dioxide (SC-CO2) extraction with ethanol and water as a modifier. The solubility of the extract was then measured before correlating using Chrastil, del Valle & Aguilera (dVA), and Adachi-Lu (A-L) models. This study revealed that a low T and increase in P at a constant modifier ratio would boost the anthocyanins content, contradicted with the extraction of total yield value, which is higher when increase T and low P. Meanwhile, analyzed results show that the solubility of Hibiscus sabdariffa calyces' extracts has successfully fitted the Chrastil's model with AARD of 27.72% as compared with dVA (35.42%) and A-L models (50.23%).

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